ASTM D1123-1999(2009) 卡尔·费歇尔试剂法测定发动机冷却剂浓缩物中水含量的标准试验方法

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【英文标准名称】:StandardTestMethodsforWaterinEngineCoolantConcentratebytheKarlFischerReagentMethod
【原文标准名称】:卡尔·费歇尔试剂法测定发动机冷却剂浓缩物中水含量的标准试验方法
【标准号】:ASTMD1123-1999(2009)
【标准状态】:现行
【国别】:美国
【发布日期】:1999
【实施或试行日期】:
【发布单位】:美国材料与试验协会(US-ASTM)
【起草单位】:D15.04
【标准类型】:(TestMethod)
【标准水平】:()
【中文主题词】:
【英文主题词】:enginecoolants;KarlFischer;watercontent;Enginecoolants/concentrates;Iodinereduction;KarlFischerreagentmethod--watercontent;Watercontent--chemicals
【摘要】:ThetotalapparentwaterinenginecoolantconcentrateasdeterminedbyKarlFischertitrationsconsistsofthefol-lowing:(1)waterpresentintheoriginalglycolbase;(2)wateradded(forexample,inhibitorsolutions);(3)waterofhydrationofinhibitors(forexample,Na2B4O7x00B7;5H2O);(4)waterformedinthechemicalreactionbetweenborateandethyleneglycol,producingboratediolcondensateandwater;and(5)quantitativeinterferencebythereactionofthereagentwithinhibitorssuchastetraborateorsodiumhydroxide.1.1Thesetestmethodscoverthedeterminationofthewaterpresentinneworunusedglycol-basedcoolantconcentratesusingamanual(TestMethodA)oranautomatic(TestMethodB)coulometrictitratorprocedure.1.2ManycarbonylcompoundsreactslowlywiththeFischerreagent,causingafadingendpointandleadingtohighresults.AmodifiedFischerreagentprocedureisincludedthatminimizestheseundesirableandinterferingreactions.1.3ThevaluesstatedinSIunitsaretoberegardedasstandard.Nootherunitsofmeasurementareincludedinthisstandard.1.4Thisstandarddoesnotpurporttoaddressallofthesafetyproblems,ifany,associatedwithitsuse.Itistheresponsibilityoftheuserofthisstandardtoestablishappropriatesafetyandhealthpracticesanddeterminetheapplicabilityofregulatorylimitationspriortouse.ForspecifichazardsstatementsseeSections8and16.
【中国标准分类号】:J96
【国际标准分类号】:
【页数】:5P.;A4
【正文语种】:英语